9. Preparation of Apparatus
9.1 Support the manual or automated apparatus on a level steady surface, such as a table.
9.2 Tests are to be performed in a draft-free room or compartment. Tests made in a laboratory hood or in any location where drafts occur are not to be relied upon.
NOTE 6 - A draft shield is recommended to prevent drafts from disturbing the vapors above the test cup. This shield should cover at least three sides of the test cup vicinity. Some apparatus may already include a built-in draft shield.
NOTE 7 - With some samples whose vapors or products of pyrolysis are objectionable, it is permissible to place the apparatus along with a shield into a hood, the draft of which is adjusted so that the vapors may be withdrawn without causing air currents over the test cup during the final 56°C(100°F) rise in temperature prior to the flash point.
9.3 Wash the test cup with the cleaning solvent to remove any test specimen or traces of gum or residue remaining from a previous test. If any deposits of carbon are present, they should be removed with a material such as a very fine grade of steel wool. Ensure that the test cup is completely clean and dry before using again. If necessary, flush the test cup with cold water and dry for a few minutes over an open flame or a hot plate to remove the last traces of solvent and water. Cool the test cup to at least 56°C (100°F) below the expected flash point before using.
9.4 Support the temperature measuring device in a vertical position with the bottom of the device located 6.4 more or less 0.1mm (1/4 more or less 1/50 in.) up from the bottom of the inside of the test cup and located at a point halfway between the center and the side of the test cup on a diameter perpendicular to the arc (or line) of the sweep of the test flame and on the side opposite to the test flame applicator mounting position.
NOTE8 - The immersion line engraved on the ASTM or IP thermometer will be 2 more or less 0.1mm (5/64 more or less 1/50 in.) below the level of the rim of the cup when the thermometer is properly positioned.
NOTE 9 - Some automated apparatus is capable of positioning the temperature measuring device automatically. Refer to the manufacturer's instructions for proper installation and adjustment.
9.5 Prepare the manual apparatus or the automated apparatus for operation according to the manufacturer's instructions for calibrating, checking, and operating the equipment.