ASTM D381 standard test method for gum content in fuels by jet evaporation
4. Summary of Test Method
4.1 A measured quantity of fuel is evaporated under controlled conditions of temperature and flow of air or steam. For aviation gasoline and aviation turbine fuel, the resulting residue is weighed and reported as milligrams per 100 mL. For motor gasoline, the residue is weighed before and after extracting with heptane and the results reported as milligrams per 100 mL.
5. Significance and Use
5.1 The true significance of this test method for determining gum in motor gasoline is not firmly established. It has been proved that high gum can cause induction-system deposits and sticking of intake valves, and in most instances, it can be assumed that low gum will ensure absence of induction-system difficulties. The user should, however, realize that the test method is not of itself correlative to induction-system deposits. The primary purpose of the test method, as applied to motor gasoline, is the measurement of the oxidation products formed in the sample prior to or during the comparatively mild conditions of the test procedure. Since many motor gasolines are purposely blended with nonvolatile oils or additives, the heptane extraction step is necessary to remove these from the evaporation residue so that the deleterious material, gum, may be determined. With respect to aviation turbine fuels, large quantities of gum are indicative of contamination of fuel by higher boiling oils or particulate matter and generally reflect poor handling practices in distribution downstream of the refinery.