ASTM D3237 Test Method for Lead In Gasoline By Atomic Absorption Spectroscopy
3. Summary of Test Method
3.1 The gasoline sample is diluted with methyl isobutyl ketone and the alkyl lead components are stabilized by reaction with iodine and a quaternary ammonium salt. The lead content of the sample is determined by atomic absorption flame spectrometry at 283.3 nm, using standards prepared from reagent grade lead chloride. By the use of this treatment, all alkyl lead compounds give identical response.
4. Significance and Use
4.1 This test method is used to ensure compliance of trace lead as required by federal regulation for lead-free gasoline (40 CFR part 80).